Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-09-16 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 114.282, 55.697, 68.713 |
| Unit cell angles | 90.00, 94.92, 90.00 |
Refinement procedure
| Resolution | 68.520 - 1.970 |
| R-factor | 0.16923 |
| Rwork | 0.168 |
| R-free | 0.20280 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.979 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.500 | 2.010 |
| High resolution limit [Å] | 1.970 | 1.970 |
| Rmerge | 0.090 | 0.450 |
| Number of reflections | 30411 | |
| <I/σ(I)> | 17.6 | 2 |
| Completeness [%] | 99.4 | 100 |
| Redundancy | 3.5 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 293 | 0.1M HEPES PH 7.0, 26% PEG3350, 0.2M (NH4)2SO4, 20C |
