4AGS

Leishmania TDR1 - a unique trimeric glutathione transferase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I02
Synchrotron site	Diamond
Beamline	I02
Temperature [K]	100
Detector technology	CCD
Collection date	2010-07-17
Detector	ADSC QUANTUM 315r
Spacegroup name	C 1 2 1
Unit cell lengths	197.477, 58.396, 160.385
Unit cell angles	90.00, 111.81, 90.00

Refinement procedure

Resolution	30.000 - 2.300
R-factor	0.15194
Rwork	0.149
R-free	0.20799
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.015
RMSD bond angle	1.418
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	CRANK
Refinement software	REFMAC (5.6.0119)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.800	2.420
High resolution limit [Å]	2.300	2.300
Rmerge	0.060	0.260
Number of reflections	74464
<I/σ(I)>	12.6	3.9
Completeness [%]	97.9	98.7
Redundancy	4	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1