4A97
X-ray structure of a pentameric ligand gated ion channel from Erwinia chrysanthemi (ELIC) in complex with zopiclone
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-06-02 |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 105.400, 266.830, 110.760 |
| Unit cell angles | 90.00, 109.20, 90.00 |
Refinement procedure
| Resolution | 43.468 - 3.343 |
| R-factor | 0.208 |
| Rwork | 0.205 |
| R-free | 0.25870 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2vl0 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.755 |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((PHENIX.REFINE: 1.8_1069)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 43.950 |
| High resolution limit [Å] | 3.340 |
| Rmerge | 0.110 |
| Number of reflections | 83009 |
| <I/σ(I)> | 12.8 |
| Completeness [%] | 99.6 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
