4A6A
A115V variant of dCTP deaminase-dUTPase from Mycobacterium tuberculosis in complex with dTTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-12 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.590, 179.510, 99.810 |
Unit cell angles | 90.00, 96.28, 90.00 |
Refinement procedure
Resolution | 49.420 - 2.900 |
R-factor | 0.25478 |
Rwork | 0.253 |
R-free | 0.28985 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.015 |
RMSD bond angle | 1.613 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 99.000 |
High resolution limit [Å] | 2.900 |
Rmerge | 0.180 |
Number of reflections | 43288 |
<I/σ(I)> | 7.01 |
Completeness [%] | 98.7 |
Redundancy | 3.74 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |