Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200H |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-05-18 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.470, 86.210, 152.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.260 - 2.300 |
R-factor | 0.1905 |
Rwork | 0.189 |
R-free | 0.22463 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gyc |
RMSD bond length | 0.010 |
RMSD bond angle | 1.279 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.700 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.110 | 0.470 |
Number of reflections | 34113 | |
<I/σ(I)> | 1.5 | 1.6 |
Completeness [%] | 97.1 | 87.1 |
Redundancy | 6.7 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | PEG 1000, PEG 8000, HEPES 100 MM, pH 7.0 |