3ZX2
NTPDase1 in complex with Decavanadate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.2 |
| Synchrotron site | BESSY |
| Beamline | 14.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-12-02 |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 162.920, 80.985, 165.517 |
| Unit cell angles | 90.00, 117.49, 90.00 |
Refinement procedure
| Resolution | 146.830 - 1.810 |
| R-factor | 0.17597 |
| Rwork | 0.175 |
| R-free | 0.22387 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.157 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.000 | 1.856 |
| High resolution limit [Å] | 1.810 | 1.809 |
| Rmerge | 0.060 | |
| Number of reflections | 127469 | |
| <I/σ(I)> | 13.2 | |
| Completeness [%] | 87.6 | |
| Redundancy | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4 | 3.7M NACL, 100MM NAACETAT PH 4.0 |
