3ZVV

Fragment Bound to PI3Kinase gamma

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	CCD
Collection date	2007-05-05
Detector	ADSC QUANTUM 315r
Spacegroup name	C 1 2 1
Unit cell lengths	143.488, 68.031, 106.251
Unit cell angles	90.00, 95.16, 90.00

Refinement procedure

Resolution	16.620 - 2.500
R-factor	0.1941
Rwork	0.192
R-free	0.24250
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.010
RMSD bond angle	1.080
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	BUSTER (2.9.6)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.570
High resolution limit [Å]	2.640	2.500
Rmerge	0.080
Number of reflections	35189
<I/σ(I)>	13.4
Completeness [%]	99.0
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1