3ZPG
Acinetobacter baumannii RibD, form 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2011-08-15 |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 72.998, 72.998, 201.456 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 68.630 - 1.990 |
| R-factor | 0.21508 |
| Rwork | 0.214 |
| R-free | 0.23671 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3zpc |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.288 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 51.620 | 2.100 |
| High resolution limit [Å] | 1.990 | 1.990 |
| Rmerge | 0.060 | 0.620 |
| Number of reflections | 38040 | |
| <I/σ(I)> | 24.7 | 4.1 |
| Completeness [%] | 99.5 | 97 |
| Redundancy | 13.3 | 12 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.2 M AMMONIUM SULFATE, 0.125 M SODIUM CACODYLATE, 30% W/V POLYETHYLENE GLYCOL 8000 |
