Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-03-24 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.480, 70.790, 100.510 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 11.960 - 1.820 |
R-factor | 0.16211 |
Rwork | 0.160 |
R-free | 0.20181 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bk0 |
RMSD bond length | 0.020 |
RMSD bond angle | 1.818 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.000 | 1.910 |
High resolution limit [Å] | 1.810 | 1.810 |
Rmerge | 0.060 | 0.340 |
Number of reflections | 30904 | |
<I/σ(I)> | 14.3 | 2.9 |
Completeness [%] | 98.2 | 92.1 |
Redundancy | 3.2 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 1.0M LITHIUM SULPHATE, 76MM TRIS/HCL, PH 8.5, 2.0MM FERROUS SULPHATE, 2.6MG/ML TRIPEPTIDE, 25MG/ML IPNS |