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3ZLB

Crystal structure of phosphoglycerate kinase from Streptococcus pneumoniae

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]100
Spacegroup nameP 1 21 1
Unit cell lengths40.347, 78.227, 59.033
Unit cell angles90.00, 96.34, 90.00
Refinement procedure
Resolution46.937 - 1.780
R-factor0.1475
Rwork0.145
R-free0.19210
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1vpe
RMSD bond length0.011
RMSD bond angle1.279
Phasing softwareMOLREP
Refinement softwarePHENIX ((PHENIX.REFINE: 1.8.1_1168))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]46.9301.880
High resolution limit [Å]1.7801.780
Rmerge0.0800.590
Number of reflections34968
<I/σ(I)>11.42.2
Completeness [%]100.0100
Redundancy3.73.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
130% PEG 4000, 0.2 M MGCL2, 0.1 M TRIS-HCL PH 8.6

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PDB entries from 2024-12-18

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