Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3ZJU

Ternary complex of E .coli leucyl-tRNA synthetase, tRNA(Leu) and the benzoxaborole AN3016 in the editing conformation

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-3
Synchrotron siteESRF
BeamlineID14-3
Temperature [K]100
Detector technologyCCD
Collection date2007-05-05
DetectorADSC QUANTUM 4
Spacegroup nameP 21 21 21
Unit cell lengths76.720, 120.030, 142.810
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000 - 2.400
R-factor0.21012
Rwork0.207
R-free0.26066
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1h3n
RMSD bond length0.014
RMSD bond angle1.390
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareREFMAC (5.6.0085)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]98.8002.460
High resolution limit [Å]2.4002.400
Rmerge0.0900.530
Number of reflections51648
<I/σ(I)>13.12.4
Completeness [%]98.799.2
Redundancy3.333.43
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
15.60.1 M SODIUM ACETATE AT PH 5.6, 14-18% PEG 6000 AND 200 MM NACL. CRYSTALS WERE FROZEN IN LIQUID NITROGEN USING A CRYOPROTECTING SOLUTION CONTAINING 22 % ETHYLENE GLYCOL

225158

PDB entries from 2024-09-18

PDB statisticsPDBj update infoContact PDBjnumon