3WV4
Crystal structure of VinN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-10-31 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9782 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 81.190, 109.820, 201.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.370 - 2.150 |
R-factor | 0.2039 |
Rwork | 0.202 |
R-free | 0.24490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3au9 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.710 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.370 | 2.210 |
High resolution limit [Å] | 2.150 | 2.150 |
Number of reflections | 44155 | |
Completeness [%] | 89.5 | 83.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 278 | 0.1M Tris-HCl, 0.2M sodium acetate, 30% polyethylene glycol 4000, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 278K |