3WQN

Crystal structure of Rv3378c_Y51F with TPP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13C1
Synchrotron site	NSRRC
Beamline	BL13C1
Temperature [K]	100
Detector technology	CCD
Collection date	2012-11-15
Detector	ADSC QUANTUM 315r
Wavelength(s)	1
Spacegroup name	P 43 21 2
Unit cell lengths	106.454, 106.454, 66.360
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.000 - 2.700
Rwork	0.240
R-free	0.26100
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	CNS (1.2)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.000	2.800
High resolution limit [Å]	2.700	2.700
Number of reflections	11190
<I/σ(I)>		3.6
Completeness [%]	99.7	96.8
Redundancy	7.2	7.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1