3WGW
Structure of PCNA bound to a small molecule inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Detector technology | CCD |
Collection date | 2012-03-03 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 192.173, 192.173, 192.173 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
R-factor | 0.18381 |
Rwork | 0.182 |
R-free | 0.22125 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vkx |
RMSD bond length | 0.020 |
RMSD bond angle | 2.419 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.800 |
Number of reflections | 30376 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |