3W8I
Crystal structure of CCM3 in complex with the C-terminal regulatory domain of MST4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ DW |
Temperature [K] | 95 |
Detector technology | IMAGE PLATE |
Collection date | 2011-11-03 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 69.100, 69.100, 117.570 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.120 - 2.400 |
R-factor | 0.2247 |
Rwork | 0.222 |
R-free | 0.26680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ajm |
RMSD bond length | 0.003 |
RMSD bond angle | 0.747 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.850 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.076 | 0.353 |
Number of reflections | 11764 | |
<I/σ(I)> | 27.3 | 7.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 12.8 | 12.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 0.1M Bis-Tris, 25% PEG3350, 0.3M ammonium acetate, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |