3VOA
Staphylococcus aureus FtsZ 12-316 GDP-form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-05-17 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.54 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 72.828, 49.551, 88.413 |
Unit cell angles | 90.00, 111.57, 90.00 |
Refinement procedure
Resolution | 19.995 - 1.730 |
R-factor | 0.1899 |
Rwork | 0.188 |
R-free | 0.22990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vxy |
RMSD bond length | 0.007 |
RMSD bond angle | 1.147 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.780 |
High resolution limit [Å] | 1.730 | 1.730 |
Rmerge | 0.050 | 0.149 |
Number of reflections | 29340 | |
<I/σ(I)> | 4.5 | |
Completeness [%] | 95.4 | 90.3 |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 0.2M Lithium sulfate, 0.1M Tris-HCl, 25% PEG 5000MME, 10% ethylene glycol, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |