3V92
S663A Stable-5-LOX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-C |
| Synchrotron site | APS |
| Beamline | 24-ID-C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-10-26 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97915 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.191, 202.375, 76.986 |
| Unit cell angles | 90.00, 109.91, 90.00 |
Refinement procedure
| Resolution | 41.468 - 2.740 |
| R-factor | 0.1858 |
| Rwork | 0.183 |
| R-free | 0.23840 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.669 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((phenix.refine: 1.7.2_869)) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 49.350 | 49.350 | 2.960 |
| High resolution limit [Å] | 2.740 | 6.580 | 2.740 |
| Number of reflections | 41056 | ||
| Completeness [%] | 95.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 295 | 10% tacsimate, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
