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3V44

Crystal structure of the N-terminal fragment of zebrafish TLR5

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL11-1
Synchrotron siteSSRL
BeamlineBL11-1
Temperature [K]100
Detector technologyCCD
Collection date2010-11-19
DetectorMARMOSAIC 325 mm CCD
Wavelength(s)0.9795
Spacegroup nameP 43 21 2
Unit cell lengths98.330, 98.330, 195.103
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 2.830
R-factor0.20556
Rwork0.204
R-free0.23839
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.012
RMSD bond angle1.386
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0110)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.930
High resolution limit [Å]2.8302.830
Rmerge0.0740.544
Number of reflections22951
Completeness [%]98.9
Redundancy5.35.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP727720% MPD, 0.1 M Hepes pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K

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