3UZP
crystal structure of ck1d with PF670462 from P21 crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-08-01 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9787 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.000, 72.800, 88.990 |
Unit cell angles | 90.00, 103.21, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.940 |
Rwork | 0.222 |
R-free | 0.23700 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.010 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.062 | 0.596 |
Number of reflections | 44834 | |
Completeness [%] | 98.0 | 97.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 100 mM Citrate, 1.0 M LiCl, 22.5-35% PEG6000, VAPOR DIFFUSION, HANGING DROP, temperature 277K, pH 5.0 |