3UIW
Zebrafish Grx2 (APO)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-03-12 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5418 |
Spacegroup name | H 3 2 |
Unit cell lengths | 92.552, 92.552, 167.077 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.665 - 2.601 |
R-factor | 0.1952 |
Rwork | 0.189 |
R-free | 0.25020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fls |
RMSD bond length | 0.014 |
RMSD bond angle | 1.242 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7_650) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 2.690 |
High resolution limit [Å] | 2.600 | 5.600 | 2.600 |
Rmerge | 0.073 | 0.038 | 0.555 |
Number of reflections | 8711 | ||
<I/σ(I)> | 14 | ||
Completeness [%] | 99.7 | 98 | 100 |
Redundancy | 5.4 | 5 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 298 | 0.3 M potassium sodium tartrate, 2 M ammonium sulfate, 0.1 m citrate, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 298.0K |