3U84
Crystal Structure of Human Menin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-08 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1.07819 |
Spacegroup name | P 41 |
Unit cell lengths | 139.891, 139.891, 54.146 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.941 - 2.500 |
R-factor | 0.2012 |
Rwork | 0.198 |
R-free | 0.23550 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.717 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7_650) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 100.000 | 100.000 | 2.590 |
High resolution limit [Å] | 2.500 | 5.390 | 2.500 |
Rmerge | 0.096 | 0.049 | 0.465 |
Number of reflections | 36832 | ||
<I/σ(I)> | 12 | ||
Completeness [%] | 100.0 | 99.7 | 100 |
Redundancy | 7 | 7.2 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | 1.4 M sodium acetate, pH 6.5, vapor diffusion, sitting drop, temperature 277K |