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3U5V

Crystal structure of Max-E47

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X25
Synchrotron siteNSLS
BeamlineX25
Temperature [K]100
Detector technologyCCD
Collection date2010-10-30
DetectorADSC QUANTUM 315r
Wavelength(s)1.1
Spacegroup nameI 21 21 21
Unit cell lengths37.480, 49.466, 74.100
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution23.256 - 1.700
R-factor0.2082
Rwork0.207
R-free0.23500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2ql2
RMSD bond length0.003
RMSD bond angle0.567
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASES
Refinement softwarePHENIX ((phenix.refine: 1.7_650))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]40.00040.0001.730
High resolution limit [Å]1.7004.6101.700
Rmerge0.0630.0340.647
Number of reflections7852
<I/σ(I)>32.146.52.1
Completeness [%]99.797.598.5
Redundancy8.994.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.62775% glycerol, 3.2-3.5 M sodium nitrate, 0.1 M sodium acetate anhydrous, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 277K

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