Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 2009-11-25 |
Detector | RIGAKU RAXIS IV++ |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 58.290, 58.290, 87.980 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.080 - 1.500 |
R-factor | 0.204 |
Rwork | 0.204 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.670 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Completeness [%] | 98.3 | 93.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 20% PEG3350, PH 7.5, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 298K |