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3TWQ

Crystal structure of ARC4 from human Tankyrase 2 (apo form)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-E
Synchrotron siteAPS
Beamline24-ID-E
Temperature [K]100
Detector technologyCCD
Collection date2010-07-18
DetectorADSC QUANTUM 315
Wavelength(s)0.9792
Spacegroup nameP 31 1 2
Unit cell lengths47.524, 47.524, 250.935
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution36.929 - 2.151
R-factor0.1767
Rwork0.174
R-free0.23450
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.046
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.7.1_743))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.230
High resolution limit [Å]2.1502.150
Rmerge0.1540.592
Number of reflections17759
<I/σ(I)>7.62
Completeness [%]97.296.9
Redundancy3.13.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP82930.1 M HEPES-NaOH pH 8.0, 0.2 M Li2SO4, 35% PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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