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3TWI

Variable Lymphocyte Receptor Recognition of the Immunodominant Glycoprotein of Bacillus anthracis Spores

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 23-ID-D
Synchrotron siteAPS
Beamline23-ID-D
Temperature [K]100
Detector technologyCCD
Collection date2010-03-10
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)1.033
Spacegroup nameI 2 2 2
Unit cell lengths74.809, 146.528, 209.501
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution41.880 - 2.550
R-factor0.19149
Rwork0.189
R-free0.23293
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB entries 2R6Q 2r9u
RMSD bond length0.011
RMSD bond angle1.211
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER (for MR)
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.640
High resolution limit [Å]2.5502.550
Number of reflections37042
<I/σ(I)>9.52
Completeness [%]97.399.1
Redundancy3.12.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.2629815% PEG 6000, 1.2 M LiCl, 0.1 M sodium citrate, pH 5.26, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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