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3T8V

A bestatin-based chemical biology strategy reveals distinct roles for malaria M1- and M17-family aminopeptidases

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron siteAustralian Synchrotron
BeamlineMX1
Temperature [K]100
Detector technologyCCD
Collection date2009-08-07
DetectorMAR CCD 165 mm
Spacegroup nameP 21 21 21
Unit cell lengths75.542, 108.821, 118.274
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.040 - 1.800
R-factor0.1622
Rwork0.160
R-free0.19760
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle0.990
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareBUSTER (2.8.0)
Data quality characteristics
 Overall
Low resolution limit [Å]46.570
High resolution limit [Å]1.800
Number of reflections90083
Completeness [%]99.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.529822%(v/v) PEG8000, 10%(v/v) Glycerol, 0.1M Tris, 0.2M MgCl2, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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