Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3SXN

Mycobacterium tuberculosis Eis protein initiates modulation of host immune responses by acetylation of DUSP16/MKP-7

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 4A
Synchrotron sitePAL/PLS
Beamline4A
Temperature [K]100
Detector technologyCCD
Collection date2010-11-08
DetectorADSC QUANTUM 315r
Wavelength(s)1.0000
Spacegroup nameP 21 21 21
Unit cell lengths107.737, 126.518, 238.800
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution19.997 - 2.030
R-factor0.1817
Rwork0.181
R-free0.21720
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.191
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASES
Refinement softwarePHENIX ((phenix.refine: 1.6.4_486))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.060
High resolution limit [Å]2.0302.030
Rmerge0.0600.390
Number of reflections203855
<I/σ(I)>36.9
Completeness [%]96.396
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.6297100mM sodium chloride, 100mM citrate, 12% PEG 4000, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 297K

217705

PDB entries from 2024-03-27

PDB statisticsPDBj update infoContact PDBjnumon