3SIL
SIALIDASE FROM SALMONELLA TYPHIMURIUM
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7B |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-05-01 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 47.100, 81.730, 91.500 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 1.050 |
| R-factor | 0.1163 |
| R-free | 0.14740 |
| Starting model (for MR) | 2sil |
| RMSD bond length | 0.014 |
| RMSD bond angle | 0.030 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 11.000 | 1.150 |
| High resolution limit [Å] | 1.050 | 1.050 |
| Rmerge | 0.056 | 0.346 |
| Number of reflections | 148478 | |
| <I/σ(I)> | 8.5 | 3.4 |
| Completeness [%] | 90.1 | 89.8 |
| Redundancy | 3.6 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.86 | pH 7.86 |
