3SFU
crystal structure of murine norovirus RNA dependent RNA polymerase in complex with ribavirin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 277 |
Detector technology | CCD |
Collection date | 2010-04-14 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 119.952, 196.084, 109.206 |
Unit cell angles | 90.00, 114.12, 90.00 |
Refinement procedure
Resolution | 47.848 - 2.501 |
R-factor | 0.1824 |
Rwork | 0.181 |
R-free | 0.22890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.141 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.093 |
Number of reflections | 78946 |
<I/σ(I)> | 21.41 |
Completeness [%] | 100.0 |
Redundancy | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 277 | 1.26M ammonium sulphate, CHES (pH 9.5), 0.2M NaCl, VAPOR DIFFUSION, HANGING DROP, temperature 277K |