3S94
Crystal structure of LRP6-E1E2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-05 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.540, 144.510, 70.760 |
Unit cell angles | 90.00, 96.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.800 |
R-factor | 0.24008 |
Rwork | 0.237 |
R-free | 0.29611 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ijq |
RMSD bond length | 0.007 |
RMSD bond angle | 1.276 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.800 |
Number of reflections | 34730 |
Completeness [%] | 100.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 80mM sodium citrate pH 5.5, 20-21% PEG3350, 40mM KSCN, VAPOR DIFFUSION, HANGING DROP, temperature 298K |