3RSM
Crystal structure of S108C mutant of PMM/PGM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Collection date | 2010-05-17 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.034, 72.806, 92.997 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.840 - 2.100 |
R-factor | 0.21463 |
Rwork | 0.213 |
R-free | 0.25252 |
Structure solution method | refinement |
Starting model (for MR) | 1k35 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.387 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.843 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.060 | 0.513 |
Number of reflections | 29767 | |
<I/σ(I)> | 11 | 2.3 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 4.8 | 4.72 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 1.4 Na,K tartrate, 100 mM Na Hepes, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |