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3QUP

Inhibitor bound structure of the kinase domain of the murine receptor tyrosine kinase TYRO3 (Sky)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Temperature [K]200
Detector technologyCCD
Collection date2005-06-25
DetectorADSC QUANTUM 210r
Wavelength(s)1.000
Spacegroup nameP 1 21 1
Unit cell lengths46.986, 57.343, 60.562
Unit cell angles90.00, 100.30, 90.00
Refinement procedure
Resolution41.310 - 1.900
R-factor0.23893
Rwork0.238
R-free0.26225
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.013
RMSD bond angle1.431
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.780
High resolution limit [Å]1.7201.720
Number of reflections30181
<I/σ(I)>30.6
Completeness [%]89.348.1
Redundancy3.52.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP729517% PEG 3350, 0.1M magnesium nitrate, 0.1 M Bis-Tris, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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