3Q2G
Adamts1 in complex with a novel N-hydroxyformamide inhibitors
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E DW |
| Temperature [K] | 100 |
| Collection date | 2005-12-05 |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.309, 63.419, 114.912 |
| Unit cell angles | 90.00, 89.88, 90.00 |
Refinement procedure
| Resolution | 114.710 - 2.300 |
| R-factor | 0.21071 |
| Rwork | 0.208 |
| R-free | 0.26068 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2jih |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.234 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 114.710 | 2.420 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Number of reflections | 31938 | |
| Completeness [%] | 96.8 | 96.1 |
| Redundancy | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
