3PZ5
The crystal structure of AaLeuRS-CP1-D20
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Detector technology | CCD |
Collection date | 2009-07-10 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | I 41 |
Unit cell lengths | 106.143, 106.143, 81.779 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.530 - 2.500 |
R-factor | 0.2151 |
Rwork | 0.213 |
R-free | 0.26610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1h3n |
RMSD bond length | 0.006 |
RMSD bond angle | 0.989 |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 15748 | |
Completeness [%] | 79.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 30 % PEG 4000, 0.1 M sodium citrate tribasic dihydrate at pH 5.6 and 0.2 M ammonium acetate , VAPOR DIFFUSION, SITTING DROP, temperature 293K |