3PVM

Structure of Complement C5 in Complex with CVF

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Detector technology	CCD
Collection date	2010-03-12
Detector	ADSC QUANTUM 315r
Spacegroup name	P 2 2 21
Unit cell lengths	176.520, 179.200, 389.690
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.469 - 4.300
R-factor	0.2336
Rwork	0.233
R-free	0.26230
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	PDB ENTRIES 3CU7 and 3HRZ
RMSD bond length	0.012
RMSD bond angle	1.535
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.6.4_486))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.469
High resolution limit [Å]	4.300	4.300
Number of reflections	79835
<I/σ(I)>	10.9	3.1
Completeness [%]	94.2	96
Redundancy	5.6	5.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1