3PB3
Structure of an Antibiotic Related Methyltransferase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X8C |
| Synchrotron site | NSLS |
| Beamline | X8C |
| Collection date | 2009-09-24 |
| Spacegroup name | P 43 |
| Unit cell lengths | 64.419, 64.419, 108.499 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.900 |
| R-factor | 0.2137 |
| Rwork | 0.212 |
| R-free | 0.24080 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.090 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 1.970 |
| High resolution limit [Å] | 1.900 | 4.090 | 1.900 |
| Rmerge | 0.084 | 0.060 | 0.353 |
| Number of reflections | 35024 | ||
| <I/σ(I)> | 17 | ||
| Completeness [%] | 100.0 | 99.7 | 100 |
| Redundancy | 12.1 | 12 | 11.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
