3O4P
DFPase at 0.85 Angstrom resolution (H atoms included)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7B |
| Detector technology | IMAGE PLATE |
| Collection date | 2000-04-01 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 0.842 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 43.114, 81.849, 86.467 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.800 - 0.850 |
| Rwork | 0.103 |
| R-free | 0.12100 |
| Starting model (for MR) | DFPase model furnished by J. Koepke. |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | MoPro |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.800 |
| High resolution limit [Å] | 0.850 |
| Number of reflections | 264548 |
| Completeness [%] | 93.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | pH 6.5 |
