Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-04-01 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 43 |
| Unit cell lengths | 123.110, 123.110, 210.010 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.294 - 2.900 |
| R-factor | 0.20975 |
| Rwork | 0.208 |
| R-free | 0.24080 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1inl |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.565 |
| Refinement software | REFMAC (5.6.0070) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.970 |
| High resolution limit [Å] | 2.850 | 2.850 |
| Rmerge | 0.087 | 0.391 |
| Number of reflections | 69092 | |
| <I/σ(I)> | 20.975 | |
| Completeness [%] | 95.3 | 94.7 |
| Redundancy | 10.6 | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 1.5M LiSO4, 0.1M Na Hepes, pH7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
