3O0J
PDE4B In complex with ligand an2898
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PILATUS |
| Wavelength(s) | 0.918 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 53.611, 53.611, 229.014 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 57.260 - 1.950 |
| R-factor | 0.1867 |
| Rwork | 0.184 |
| R-free | 0.23650 |
| Structure solution method | OTHER |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.065 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 57.260 | 2.030 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.058 | 0.383 |
| Number of reflections | 25081 | |
| Completeness [%] | 98.3 | 85.1 |
| Redundancy | 11.6 | 4.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | hanging drop vapor diffusion | 7.4 | 298 | MgCl2, pH 7.4, hanging drop vapor diffusion, temperature 298K |
