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3NZX

Crystal structure of the yeast 20S proteasome in complex with ligand 2c

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyCCD
Collection date2009-11-04
DetectorMAR CCD 165 mm
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths134.200, 300.110, 143.630
Unit cell angles90.00, 112.60, 90.00
Refinement procedure
Resolution15.000 - 2.700
R-factor0.227
Rwork0.226
R-free0.24800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ryp
RMSD bond length0.007
RMSD bond angle1.400
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.600
High resolution limit [Å]2.5002.500
Rmerge0.0850.533
Number of reflections359106
<I/σ(I)>10.12.5
Completeness [%]99.699.7
Redundancy2.62.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.8293100 mM MES/Hcl, pH 6.8, 20 mM MGAc2, 12 % MPD, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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