3NSP
Crystal structure of tetrameric RXRalpha-LBD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | IMAGE PLATE |
Collection date | 2009-06-03 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 114.828, 100.271, 47.157 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.900 |
R-factor | 0.22627 |
Rwork | 0.222 |
R-free | 0.30755 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g1u |
RMSD bond length | 0.013 |
RMSD bond angle | 1.527 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 29.720 |
High resolution limit [Å] | 2.900 |
Number of reflections | 10888 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 100mM Tris, pH6.5, 10% PEG 4000, 5% glycerol, VAPOR DIFFUSION, HANGING DROP, temperature 277K |