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3NKQ

Crystal structure of mouse autotaxin in complex with 18:3-LPA

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron sitePhoton Factory
BeamlineAR-NE3A
Temperature [K]100
Detector technologyCCD
Collection date2010-03-16
DetectorADSC QUANTUM 270
Wavelength(s)1.000
Spacegroup nameP 1 21 1
Unit cell lengths61.522, 94.528, 75.577
Unit cell angles90.00, 94.81, 90.00
Refinement procedure
Resolution25.892 - 1.700
R-factor0.1923
Rwork0.190
R-free0.22770
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3nkm
RMSD bond length0.010
RMSD bond angle1.409
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwarePHENIX (1.6_289)
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]1.700
Number of reflections94215
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP29320-25% PEG 3350, 0.15mM NaCl, 0.5M KSCN, 0.2mM ZnSO4, 1% polyvinylpyrrolidone, vapor diffusion, sitting drop, temperature 293K

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