3N0A
Crystal structure of auxilin (40-400)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-11 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 137.925, 137.925, 51.327 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.900 - 2.200 |
R-factor | 0.1734 |
Rwork | 0.172 |
R-free | 0.19950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1d5r |
RMSD bond length | 0.007 |
RMSD bond angle | 1.046 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.220 |
High resolution limit [Å] | 2.180 | 2.180 |
Rmerge | 0.082 | 0.531 |
Number of reflections | 29000 | |
<I/σ(I)> | 22.4 | 2.6 |
Completeness [%] | 99.9 | 99.4 |
Redundancy | 7.6 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 15.5% PEG 4000, 0.1 M HEPES, pH 7.5, 0.01 M CaCl2, 0.8 M NaCl, VAPOR DIFFUSION, HANGING DROP, temperature 293K |