3MYA
Crystal Structure of HP67 H41F - P61
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 200 |
Detector technology | IMAGE PLATE |
Collection date | 2009-12-18 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 61 |
Unit cell lengths | 65.409, 65.409, 68.283 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 18.900 - 2.500 |
R-factor | 0.2175 |
Rwork | 0.215 |
R-free | 0.27650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rjw |
RMSD bond length | 0.008 |
RMSD bond angle | 1.006 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.900 |
High resolution limit [Å] | 2.500 |
Number of reflections | 5554 |
Completeness [%] | 95.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2 M Ammonium Sulfate, 0.1 M 2-morpholinoethanesulfonic Acid, 30% Polyethylene Glycol 8,000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |