3MXX
Crystal structure of WDR5 mutant (S62A)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-002+ |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-03 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.629, 79.645, 45.656 |
Unit cell angles | 90.00, 102.02, 90.00 |
Refinement procedure
Resolution | 42.670 - 2.050 |
R-factor | 0.19021 |
Rwork | 0.188 |
R-free | 0.23920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2h14 |
RMSD bond length | 0.022 |
RMSD bond angle | 1.874 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASES |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.670 | 2.120 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmerge | 0.064 | 0.142 |
Total number of observations | 66969 | |
Number of reflections | 19198 | |
Completeness [%] | 99.8 | 98.9 |
Redundancy | 3.49 | 2.84 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 18% PEG 3350, 0.1M Hepes, 18mM (NH4)2SO4, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |