3MV7
Crystal Structure of the TK3 TCR in complex with HLA-B*3501/HPVG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-05 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.979457 |
Spacegroup name | P 1 |
Unit cell lengths | 44.860, 62.240, 92.560 |
Unit cell angles | 94.64, 103.92, 109.31 |
Refinement procedure
Resolution | 57.830 - 2.000 |
R-factor | 0.228 |
Rwork | 0.225 |
R-free | 0.28600 |
Structure solution method | 2FYY, 3FFC |
RMSD bond length | 0.009 |
RMSD bond angle | 1.256 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.100 | |
High resolution limit [Å] | 2.000 | 10.000 | 2.000 |
Rmerge | 0.103 | 0.030 | 0.544 |
Number of reflections | 59242 | 473 | 7954 |
<I/σ(I)> | 10.84 | 39.3 | 2.6 |
Completeness [%] | 97.0 | 96.5 | 95.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 277 | 15%PEG 3350, 0.2M LiSO4, 0.1M Na-citrate, pH 5.6, vapor diffusion, hanging drop, temperature 277K |