3MC6
Crystal structure of ScDPL1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2007-11-27 |
Detector | PSI PILATUS 6M |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 151.100, 156.860, 201.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.920 - 3.150 |
R-factor | 0.243 |
Rwork | 0.241 |
R-free | 0.30000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | REFINED MODEL OF STSPL MUTANT K311A (DIMERIC) |
RMSD bond length | 0.002 |
RMSD bond angle | 0.522 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.5_2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.990 | 3.320 |
High resolution limit [Å] | 3.150 | 3.150 |
Rmerge | 0.087 | 0.710 |
Number of reflections | 20848 | |
<I/σ(I)> | 15.1 | 2.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.52 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.7 | 293 | PEG 4000 18%, 0.1 M Na-cacodylate (HOAc) pH 6.7, 0.2 M Li2SO4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |