3M1I
Crystal structure of yeast CRM1 (Xpo1p) in complex with yeast RanBP1 (Yrb1p) and yeast RanGTP (Gsp1pGTP)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-26 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 106.209, 106.209, 303.602 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.510 - 2.000 |
R-factor | 0.178 |
Rwork | 0.175 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1rrp 1w9c 2h4m |
RMSD bond length | 0.026 |
RMSD bond angle | 2.042 |
Data reduction software | PROCESS |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.330 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.087 | 0.876 |
Number of reflections | 117954 | |
<I/σ(I)> | 5.7 | 2.9 |
Completeness [%] | 99.9 | 100 |
Redundancy | 14.2 | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.6 | 293 | 0.1M Bis-Tris, 0.2M ammonium nitrate, 18% PEG3350, pH 6.6, VAPOR DIFFUSION, SITTING DROP, temperature 293K |