3LZ6
Guinea Pig 11beta hydroxysteroid dehydrogenase with PF-877423
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.2 |
| Synchrotron site | ALS |
| Beamline | 5.0.2 |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 78.398, 83.899, 179.964 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 91.290 - 1.840 |
| R-factor | 0.2092 |
| Rwork | 0.207 |
| R-free | 0.25137 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.023 |
| RMSD bond angle | 2.085 |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 91.290 |
| High resolution limit [Å] | 1.840 |
| Number of reflections | 91639 |
| Completeness [%] | 88.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
