3LUM
Structure of ulilysin mutant M290L
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Detector technology | CCD |
Collection date | 2009-02-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.976 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 97.310, 174.110, 124.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.280 - 1.700 |
R-factor | 0.16289 |
Rwork | 0.163 |
R-free | 0.19487 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2cki |
RMSD bond length | 0.012 |
RMSD bond angle | 1.356 |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.700 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.104 | 0.196 |
Number of reflections | 115779 | |
<I/σ(I)> | 15.2 | 7.9 |
Redundancy | 9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | pH 7.5, VAPOR DIFFUSION, SITTING DROP |